Due to increasing oil prices and the obvious influence of the combustion of fossil fuel derivatives on climate change on the one hand and the steady growth of transportation needs on the other, it is necessary to develop alternatives to oil for aviation. The project Alfa Bird (Alternative Fuels and Bio-fuels in Aircraft Development) focuses on an identification of possible alternative fuels to kerosene, the investigation of the adequacy of the selected ones, an evaluation of the environmental and economic impact of them, and finally the creation of a future perspective for the industrial use of the "best" alternative. The main part of the investigation activities consists of the analysis of the evaporation of the previously chosen fuel types in comparison to fully synthetic jet fuel. Therefore qualitative measurements to obtain vapor concentration gradients will be done using the infrared extinction (IRE) measurement method. Based on a simplified Beer-Bouguer-Lambert law the integral vapor concentrations can be obtained. The main hypothesis is that if the line-of-sight extinction due to Mie-scattering is similar for both infrared and visible wavelengths because of the presence of the spray, only infrared light Mill be absorbed by the fuel vapor, being transparent to visible light. This contribution focuses on the validation of the infrared measurement technique on a well characterized spray. The tests are performed under controlled boundary conditions. Therefore an existing IRE test arrangement at ONERA Toulouse using an ultrasonic atomizer injecting n-octane at atmospheric conditions has been analyzed. Error sources related to misalignments in the hardware have been considered and an iterative alignment method of the laser beams followed by a beam diameter and diffraction analysis have been performed. Optimizing the setup to obtain a stable operation point has been successful. Improved experimental results at this operation point were compared with existing simulation results for the evaporation of the ultrasonic atomizer used. The achieved data has shown good accordance to the existing simulation results.